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GCMS analysis results for sample AD29664, Jan 2002

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Gas chromatography-mass spectrometry analysis of sample AD29664 conducted January 9, 2002, reporting unknown compounds and surrogate recovery at 78%.

NYC-WTC_000037188–000037196

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1401\29664.D Vial: 16 Acq On : 15 Dec 2001 5:10 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 15 17:59 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.03 178 442 N.D. 34) Anthracene 25.03 178 442 N.D. 35) Di-n-butylphthalate 27.00 149 9349 N.D. 36) Fluoranthene 28.70 202 102 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.50 149 1645 N.D. 41) Benzo(a)anthracene 33.01 228 4641 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 33530 0.40 ug/1 96 43) Chrysene 33.01 228 4641 N.D. 45) Di-n-Octylphthalate 35.04 149 1404 N.D. 46) Benzo(b)fluoranthene 36.14 252 791 N.D. 47) Benzo(k)fluoranthene 36.14 252 880 N.D. 4 8) Benzo(a)pyrene 36.94 252 216 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29664.D GCMS1126.M Fri Dec 28 12:50:29 2001 Page 2

NYC-WTC_000037191

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NYC-WTC_000037191Source: NYC Law Department, mirrored locally

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