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GCMS comments for sample AD29785 detecting phthalate, Jan 2002

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Laboratory commentary noting a GCMS scan of sample AD29785 revealing bis(2-Ethylhexyl)phthalate on January 7, 2002.

NYC-WTC_000037071–000037082

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1401\29785.D Vial: 5 Acq On : 15 Dec 2001 6:26 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 15 7:15 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.04 178 459 N.D. 34) Anthracene 25.04 178 459 N.D. 35) Di-n-butylphthalate 27.00 149 18223 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.01 228 4838 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 24390 0.29 ug/1 100 43) Chrysene 33.09 228 2033 N.D. 45) Di-n-Octylphthalate 35.02 149 767 N.D. 46) Benzo(b)fluoranthene 36.12 252 2735 N.D. 47) Benzo(k)fluoranthene 36.12 252 2735 N.D. 48) Benzo(a)pyrene 36.95 252 52.9 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29785.D GCMS1126.M Wed Jan 02 09:14:57 2002 Page 2

NYC-WTC_000037074

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NYC-WTC_000037074Source: NYC Law Department, mirrored locally

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