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GCMS analysis results for sample AD29187, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD29187 conducted on January 4, 2002, by the DEP.

NYC-WTC_000037116–000037125

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1401\29187.D Vial: 19 Acq On : 15 Dec 2001 8:05 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 15 20:54 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.04 178 1741 N.D. 34) Anthracene 25.18 178 844 N.D. 35) Di-n-butylphthalate 26.99 149 59643 0.30 ug/1 # 97 36) Fluoranthene .28.68 202 1036 N.D. 3 9) Pyrene 29.34 202 1150 N.D. 40) Butylbenzylphthalate 31.50 149 306 N.D. 41) Benzo(a)anthracene 33.00 228 6238 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 13850 N.D. 43) Chrysene 33.00 228 6238 N.D. 45) Di-n-Octylphthalate 35.04 149 426 N.D. 46) Benzo(b)fluoranthene 36.08 252 237 N.D. 47) Benzo(k)fluoranthene 36.11 252 898 N.D. 48) Benzo(a)pyrene 36.94 252 106 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29187.D GCMS1126.M Fri Dec 28 12:52:25 2001 Page 2

NYC-WTC_000037119

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NYC-WTC_000037119Source: NYC Law Department, mirrored locally

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