NYC-WTC_000017958
Laboratory report documenting GCMS analysis of sample AD30489 conducted on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 11 pages
GCMS analysis results for sample AD30473, Jan 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of sample AD30473 conducted on January 24, 2002.
NYC-WTC_000017969–000017979Folder label: “GCMS X 12/14/01 A 12/31/01”
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\DEC3101\30473.D . Vial: 14 Acq On : 31 Dec 2001 11:37 pm Operator: 209 GALOS Sample : gems scan 12/14fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 23 8:10 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update ' : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.68 152 789032m 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3090500m 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 1648875 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 2319057 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 1437200 20.00 ug/1 -0.01 44) Perylene-dl2 37.12 264 770518 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.07 235 135545 5.32 ug/mL 0.00 Spiked Amount 5.000 Recovery = 106.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.35 74 112 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 11.59 146 5320 N.D. 5) 1,4-Dichlorobenzene 11.72 146 7091 N.D. 6) 1,2-Dichlorobenzene 12.25 146 3689 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 13.07 117 3138 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 15.19 180 1600 N.D. 15) Naphthalene 15.34 128 4021 N.D. 16) Hexachlorobutadiene 15.90 225 3095 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 20.65 153 728 N.D. 24) 2,4-Dinitrotoluene 21.25 165 291 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 30473.D GCMS1126.M Wed Jan 23 08:11:30 2002 Page 1
NYC-WTC_000017971
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