GCMS analysis results for sample AD30471, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30471 conducted on January 24, 2002.

NYC-WTC_000017922–000017930

Folder label: “GCMS X 12/14/01 A 12/31/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC3101\30471.D Vial: 10 Acq On : 31 Dec 2001 7:44 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 20:33 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.67 152 840208 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3277946 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.57 164 1698328 20.00 ug/1 0.00 29) Phenanthrene-diO 24.98 188 2444455 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 1455061 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 798799 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.07 235 131578 4.90 ug/mL 0.00 Spiked Amount 5.000 Recovery = 98.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.21 74 277 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. % 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 648 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 . 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 . N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.19 165 175 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 30471.D GCMS1126.M Tue Jan 15 11:20:44 2002 Page 1

NYC-WTC_000017924

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NYC-WTC_000017924Source: NYC Law Department, mirrored locally

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