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GCMS unknowns analysis report for sample AD29931, Jan 2002

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Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD29931 using GCMS on January 18, 2002.

NYC-WTC_000017060–000017068

Folder label: “GCMS X 12/14/01 A 1/1/02

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NYC 9/11 Public Portal Document a Quantitation Report (QT Reviewed) i. Data File : C:\HPCHEM\1\DATA\DEC3101\29931.D Vial: 17 Acq on : 1 Jan 2002 2:31 am Operator: 209 GALOS Sample : gems scan 12/l4a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 1 3:20 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcg Meth : GCMS1126 Internal Standards R.T. QIon Response Cone Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.68 152 875207 20.00 ug/l -0.02 10) Naphthalene-ds 15.27 136 3415571 20.00 ug/l = -0.03 17) Acenaphthene-d10 20.56 164 1782829 20.00 ug/l = -0.01 29) Phenanthrene-d10 24.99 188 2515069 20.00 ug/1 0.00 38) Chrysene-di2 33.03 240 1495269 20.00 ug/l 0.00 44) Perylene-d12 37.12 264 847401 20.00 ug/1 0.00 System Monitoring Compounds 37) 2,4-DDD 30.06 235 135533 4.90 ug/ml 0.00 Spiked Amount 5.000 Recovery = 98.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.20 74 614 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 ° N.D. 6) 1,2-Dichlorobenzene 0.00 146 C) N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0) N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0) N.D. 9) Hexachloroethane 0.00 117 ° N.D. 11) Nitrobenzene 0.00 «77 0 N.D. 12) Isophorone 0.00 82 0) N.D. 13) bis(2-Chloroethoxy) methane 0.00 93 0) N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0) N.D. 15) Naphthalene 15.34 128 875 N.D. 16) Hexachlorobutadiene 0.00 225 ° N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0) N.D. 20) Dimethylphthalate 0.00 163 0) N.D. 21) 2,6-Dinitrotoluene 0.00 165 ° N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 ° N.D. 24) 2,4-Dinitrotoluene 21.24 165 285 N.D. 25) Diethylphthalate 22.18 149 365 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 CO) N.D. (#) = qualifier out of range (m) = manual integration 29931.D GCMS1126.M Tue Jan 15 12:20:52 2002 Page 1 NYC-WTC_000017062

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NYC-WTC_000017062Source: NYC Law Department, mirrored locally

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