NYC-WTC_000016970
Laboratory report detailing GCMS analysis of sample AD31345 conducted on February 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 11 pages
GCMS analysis results for sample AD30486, Jan 2002
Machine-extracted title · confidence 100%Laboratory report detailing GCMS analysis of sample AD30486 including DDD surrogates on January 18, 2002.
NYC-WTC_000017097–000017107Folder label: “GCMS X 12/14/01 A 1/1/02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
' Data File C:\HPCHEM\1\DATA\DEC3101\30486.D Vial: 21 . Acq On 1 Jan 2002 6:23 am Operator: 209 GALOS Sample gems scan 12/14a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 1 7:12 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.68 152 868232 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 3369222 20.00 ug/1 -0.03 17) Acenaphthene-dl0 20.56 164 1727786 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 2441859 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 1403631 20.00 ug/1 -0.01 44) Perylene-dl2 37.12 264 791420 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.07 235 115091 4.29 ug/mL 0.00 Spiked Amount 5.000 Recovery = 85.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.21 74 308 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachl oroe thane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 2040 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.05 165 1240 N.D. 25) Diethylphthalate 22.18 149 187 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration 30486.D GCMS0103.M Tue Jan 15 14:24:29 2002 Page 1
NYC-WTC_000017099
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