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GCMS unknowns analysis report for sample AD31275, Feb 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31275 using GCMS on February 11, 2002.

NYC-WTC_000016992–000017003

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000017000
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NYC 9/11 Public Portal Document i Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\JAN0902\31275.D Vial: 9 Acq On : 10 Jan 2002 11:22 pm Operator: 209 GALOS Sample = gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSIE SII IIIS IIIS IIIS IO IIE IS IOI TOTO III III II II II Peak Number 2 2-Butanol, 3,3'-oxybis- Concentration Rank 3 R.T, EstCone Area Relative to ISTD Ret. 11.22 0.41 ug/1 89653 1, 4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 2-Butanol, 3,3/-oxybis- 162 C8H1803 054305-61-2 64 2 1-Propanol, Z-(2-hydroxypropoxy)- 134 C6H1403 000106-62-7 59 3 2-Propanol /1-(2-methoxy-1-methylet 148 C7H1603 020324-32-7 56 4 2-Propano¥, 1,1'-oxybis-__ ____134 C6H1403 000110-98-5 56 Abundance Sean 872 14.297 ning STAVE Yaz BB.05 109.00 . | 5000. | - 103 . Fr 8 10.80_11.00 11.20 11.40 11.60 oor z 95 : as be we ee | 44-95, 59-68 Abundanos al 2Butandi, 33 aHbs- | Cae 74s | 103 “s0'80_11'00_1120 1140 7160 | m/z 103.05, 32.31 134 mz _20 30 40 50 60 70 0 90 100 110 120 130 140 ‘Abundancs TE gee pa 59 40180 11:00 11.20 41.40. 11.60 5000 [m/z 41.05 28.64 st 45 103 75 a9 : miz> __20__30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- " { 10.80 11.00 11.20 11.40 11.60. ] m/z 73.00 25.43 5000: | . | Ss | a 1 \ 31 | / 130 mz-> 20 30 408060708 e100 140 120130” 140 | 1080 11.00 1120 1140 1160 31275.D GCMS0103.M Tue Feb 05 16:50:32 2002 Page 2 NYC-WTC_000017000

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NYC-WTC_000017000Source: NYC Law Department, mirrored locally

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