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GCMS unknowns analysis report for sample AD31275, Feb 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31275 using GCMS on February 11, 2002.

NYC-WTC_000016992–000017003

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000016999
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NYC 9/11 Public Portal Document : Library Search Compound Report 5 Data File : C:\HPCHEM\1\DATA\JAN0902\31275.D Vial: 9 Acq On : 10 Jan 2002 11:22 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSE OIG ISIS IIIS IOI ISS IO ISI IOI IO III IO IIIT III III SAI IIA Peak Number 1 Silane, tetramethyl- Concentration Rank 1 R.T. EstCone Area Relative to ISTD R.T. 7.47 3.68 ug/l 796030 1,4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Silane, teframethyl- 88 C4Hi2si 000075-76-3 9 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 5 3 N-Ethyl formamide 73 C3H7NO 000627-45-2 5 _4 Formic acid, ethyl ester 74_C3H602 000109-94-4 4 ‘Bbundancs sia 2 m/z 73.00 100.00% 43 , 720 "740 7.60 7.80 Rll St oe 8 a oo w/a 43.05 32.118 me->__10 20 304080 708090100110. | Abundance #62832; Silane, ak 5000. 720 7.40. 7.60 7.80 aq m/z 41.0 11.94% 18 183. 59 86 mi> __ 10 2030400607080 100110 30 7.20 740 7.60 7.80 5000: | m/z 45.0 11.89% | | | 15 41 65 70 87 | mz-> __ 10.20 3040 506070 oa 100. 10 | Abundance W2e2: NEthytformamide eal 7.20 7.40 7.60 7.80 ? m/z 71.00 6.79) 4 58 | | 15, | | me> 10 20 30 40806070 100.110 120740. 7.80 7.80 31275.D GCMS0103.M Tue Feb 05 16:50:27 2002 Page 1 NYC-WTC_000016999

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NYC-WTC_000016999Source: NYC Law Department, mirrored locally

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