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GCMS unknowns analysis report for sample AD31276, Feb 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31276 using GCMS on February 11, 2002.

NYC-WTC_000016961–000016969

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000016968
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NYC 9/11 Public Portal Document F Library Search Compound Report : Data File : C:\HPCHEM\1\DATA\JAN0902\31276.D Vial: 14 Acq On, : 11 dan 2002 4:15 am Operator: 209 GALOS Sample : gems scan 12/24 Inst. : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS ISI IGS ISSO IIS SS I IDE IOS IOSEI IOI III SO ISIS ISOS ITE Peak Number 1 Silane, tetramethyl- Concentration Rank 1 R.T. EstCone Area Relative to ISTD R.T. 7.46 4.75 ug/l 940076 1,4-Dichlorobenzene-d4 11.52 Hit# of 5 Tervitative ID MW MolForm cas# Qual 1 Silane, tetyYamethyl- 88 C4H12Si 000075-76-3 9 2 N-Ethylfoyfamide 73 C3H7NO 000627-45-2 9 3 Pentane, /3-methoxy- 102 CéH140 036839-67-5 9 4 1-Butanémine, 3-methyl~- _,~——_-87_CSHI3N_____000107-85-7 7 ‘Rourdancs ‘Sean 264 (7-468 min): S127ED () m/z 72.95 100.008 1 | 5000 43 , 55 a 7.20 7.40. 7.80 _ 7.80 reeey 10, 00, Kihlep preter | mz «43.05 32.21 mz> "10" "20 "304050 eo 70 go 8800110 | Abundance #62932: Silane, tetramethyl 5000 : —-1.20_7.40__7.60_7.8 as m/z 41.00 12.29 15 5359 88 mz->___10 203040 g0 gO go 10010 ‘Abundance: #292: NEE ylornaniide 30 3 5 i 7.20 7.40 7.60 7.80 5000: | m/z 44.9! 11.76 44 88 i 115 i | ene nes eee miz> 10.20 30 40 50 60 - 70 8 0 100 110 Abundance #1793: Pentane, 3-methoxy- i 7207.40 7.80 _ 7.80 m/z 71.00 7.29 os j 45 | | 27 43 39) 55 mz" “t0" "20" '90 "so "0" "60" 7060.90" 10040 | "7.20740" 7.60 7.80 31276.D GCMS0103.M Tue Feb 05 16:51:25 2002 Page 1 NYC-WTC_000016968

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NYC-WTC_000016968Source: NYC Law Department, mirrored locally

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