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GCMS analysis report for sample AD30257, January 2002

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Laboratory GCMS analysis report for sample AD30257 conducted on January 9, 2002, by analyst DLV.

NYC-WTC_000016764–000016772

Folder label: “GCMS X 12/12/01 A 12/19/01

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NYC 9/11 Public Portal Document Lor Quantitation Report (QT Reviewed) . Data File : C:\HPCHEM\1\DATA\DEC3101\30257.D Vial: 57 Acq On : 2 dan 2002 9:12 pm Operator: 209 GALOS Sample : gems scan 12/12 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 2 22:00 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update |: Fri Dec 28 15:11:00 2001 ' Response via : Initial Calibration DataAcq Meth : GCMS1126 Internal Standards R.T. QIon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.67 152 750040 20.00 ug/l -0.03 10) Naphthalene-ds 15.28 136 2874565 20.00 ug/l -0.03 17) Acenaphthene-d10 20.57 164 1432532 20.00 ug/1 0.00 29) Phenanthrene-d10 24.99 188 2141502 20.00 ug/1 0.00 38) Chrysene-d12 33.02 240 1268432 20.00 ug/1 0.00 44) Perylene-d12 37.12 264 679586 20.00 ug/l 0.00 System Monitoring Compounds 37) 2,4-DDD 30.07 235 100786 4.28 ug/mL 0.00 Spiked Amount 5.000 Recovery = 85.60% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.22 74 262 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 ° N.D. 4) 1,3-Dichlorobenzene 11.62 146 192 N.D. 5) 1,4-Dichlorobenzene 11.73 146 191 N.D. * 6) 1,2-Dichlorobenzene 12.25 146 171 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0) N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 ° N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 ° N.D. 15) Naphthalene 15.33 128 3324 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 ° N.D. 19) 2-Chloronaphthalene 0.00 162 C) N.D. 20) Dimethylphthalate 0.00 163 ° N.D. 21) 2,6-Dinitrotoluene 0.00 165 ° N.D. 22) Acenaphthylene 20.15 152 528 N.D. 23) Acenaphthene 20.66 153 517 N.D. ‘ 24) 2,4-Dinitrotoluene 21.13. 165 316 N.D. 25) Diethylphthalate 22.20 149 223 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 fe) N.D. (#) = qualifier out of range (m) = manual integration 30257.D GCMS1126.M Thu Jan 03 09:55:07 2002 Page 1 | NYC-WTC_000016766

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NYC-WTC_000016766Source: NYC Law Department, mirrored locally

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