NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\JAN0302\30118.D Vial: 11
Acq On 3 Jan 2002 8:20 pm Operator: 209 GALOS
Sample gems scan 12/12 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY-P
Quant Time: Jan 7 10:45 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update •: Fri Dec 28 15:11:00 2001
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.52 152 930553 20.00 ug/1 -0.18
10) Naphthalene-d8 15.12 136 3580354 20.00 ug/1 -0.19
17) Acenaphthene-diO 20.39 164 1765164 20.00 ug/1 -0.19
29) Phenanthrene-diO 24.81 188 2642874 20.00 ug/1 -0.19
38) Chrysene-dl2 32.84 240 1574413m 20.00 ug/1 -0.19
44) Perylene-dl2 36.91 264 921903 20.00 ug/1 -0.21
System Monitoring Compounds
37) 2,4-DDD 29.88 235 138904 4.78 ug/mL -0.19
Spiked Amount 5.000 Recovery = 95.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.20 74 102 N.D.
3) bis(2-Chloroethyl)ether 11.01 93 687 N.D.
4) 1,3-Dichlorobenzene 11.44 146 692 N.D.
5) 1,4-Dichlorobenzene 11.58 146 652 N.D.
6) 1,2-Dichlorobenzene 12.10 146 604 N.D.
7) 2,2' -oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 13.33 77 179 N.D.
12) 1sophorone 13.91 82 675 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.19 128 2635 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 19.80 163 1286 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
2 2) Acenaphthylene 19.94 152 197 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 20.86 165 708 N.D.
25) Diethylphthalate 21.91 149 2518 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30118.D GCMS0103.M Mon Jan 07 10:45:56 2002 Page 1
NYC-WTC_000016785
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