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GCMS sample analysis report, Feb 2002

Machine-extracted title · confidence 80%

Gas chromatography mass spectrometry report documenting analytical results for environmental samples processed in mid-February 2002.

NYC-WTC_000016667–000016679

Folder label: “GCMS X 12/31/01 A 1/18/02

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Scanned page image, NYC-WTC_000016672
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN1802\31550.D Vial: 16 Acq On : 19 Jan 2002 6:13 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.447 258 262 295 rVB 321332 985980 16.33% 3.079% 2 11.495 698 703 724 rBV 1773224 4745076 78.61% 14.817% 3 15.094 1089 1095 1110 rBV 2792398 5910297 97.91% 18.455% 4 20.354 1662 1668 1692 rBV 2934029 6036522 100.00% 18.850% 5 24.522 2117 2122 2127 rBV 38064 71000 1.18% 0.222%

6 24.770 2143 2149 2162 rBV2 2597541 5661580 93.79% 17.679% 7 25.807 2258 2262 2270 rVB 62853 129411 2.14% 0.404% 8 27.047 2390 2397 2404 rBV 67273 143084 2.37% 0.447% 9 28.222 2519 2525 2531 rBV 47632 106592 1.77% 0.333% 10 29.847 2697 2702 2709 rVB 340235 689845 11.43% 2.154%

11 32.803 3017 3024 3043 rBV2 1805581 4285484 70.99% 13.382% 12 33.106 3052 3057 3068 rVB 32664 98113 1.63% 0.306% 13 36.861 3459 3466 3481 rBV 1164274 3161615 52.37% 9.872%

Sum of corrected areas: 32024599

31550.D GCMS0103.M Wed Feb 06 15:40:42 2002

NYC-WTC_000016672

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NYC-WTC_000016672Source: NYC Law Department, mirrored locally

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