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GCMS analysis results for sample AE00008, Feb 13 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00008 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050109–000050121

Folder label: “GCMS X 1/3/02 A 1/24/02

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Scanned page image, NYC-WTC_000050114
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN2402\8.D Vial: 10 Acq On : 24 Jan 2002 9:53 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.432 256 260 272 rBV 376417 957984 13.43% 2.552% 2 7.570 272 275 293 rVB 46543 185307 2.60% 0.494% 3 11.178 663 668 673 rBV 31840 75561 1.06% 0.201% 4 11.260 673 677 684 rVB 30929 74142 1.04% 0.197% 5 11.481 697 701 719 rBV 2186974 5576141 78.17% 14.852%

6 14.134 984 990 996 rBV 207857 407021 5.71% 1.084% 7 15.079 1087 1093 1111 rBV 3463773 6980091 97.85% 18.592% 8 20.340 1660 1666 1691 rBV 3386895 7133570 100.00% 19.000% 9 24.755 2141 2147 2159 rBV2 3115493 6736548 94.43% 17.943% 10 29.832 2695 2700 2708 rBV 421385 838358 11.75% 2.233%

11 32.779 3015 3021 3040 rBV2 1997927 4779070 66.99% 12.729% 12 36.846 3456 3464 3488 rBV2 1406728 3800617 53.28% 10.123%

Sum of corrected areas: 37544410

8.D GCMS0208.M Fri Feb 08 13:42:31 2002

NYC-WTC_000050114

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NYC-WTC_000050114Source: NYC Law Department, mirrored locally

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