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GCMS analysis results for sample AE00102, Feb 13 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00102 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050099–000050108

Folder label: “GCMS X 1/3/02 A 1/24/02

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Scanned page image, NYC-WTC_000050104
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN2402\102.D Vial: 9 Acq On : 24 Jan 2002 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.439 257 261 295 rVB 354494 1016176 13.80% 2.706% 2 11.487 697 702 725 rBV 2399045 5656046 76.80% 15.063% 3 14.131 984 990 997 rBV 317698 602405 8.18% 1.604% 4 15.077 1088 1093 1111 rBV 3453455 7164252 97.28% 19.080% 5 20.346 1660 1667 1686 rBV . 3523221 7364859 100.00% 19.614%

6 24.753 2141 2147 2160 rBV2 3101519 6888446 93.53% 18.345% 7 29.829 2695 2700 2707 rBV 412434 827480 11.24% 2.204% 8 32.785 3015 3022 3049 rBV 1975619 4585140 62.26% 12.211% 9 36.843 3456 3464 3484 rBV 1255688 3444117 46.76% 9.172%

Sum of corrected areas: 37548921

102 .D GCMS0208.M Fri Feb 08 13:36:59 2002

NYC-WTC_000050104

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NYC-WTC_000050104Source: NYC Law Department, mirrored locally

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