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GCMS analysis results for sample AE00009, Feb 13 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00009 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050122–000050134

Folder label: “GCMS X 1/3/02 A 1/24/02

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Scanned page image, NYC-WTC_000050127
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\JAN2402\9.D Vial: 11 Acq On : 24 Jan 2002 10:52 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.440 257 261 273 rBV 408584 1026150 12.15% 2.327% 2 7.577 273 276 293 rVB 30194 136580 1.62% 0.310% 3 11.158 663 666 672 rBV 154282 334438 3.96% 0.759% 4 11.240 672 675 684 rVB 170236 385736 4.57% 0.875% 5 11.488 695 702 721 rBV2 2819776 6963246 82.43% 15.793%

6 14.132 984 990 995 rBV 136615 263113 3.11% 0.597% 7 15.078 1088 1093 1112 rBV 4028848 8190814 96.96% 18.577% 8 20.347 1660 1667 1683 rBV 3950577 8447704 100.00% 19.160% 9 24.754 2141 2147 2159 rBV2 3496127 7858789 93.03% 17.824% 10 29.830 2695 2700 2707 rBV 476875 969333 11.47% 2.198%

11 32.787 3015 3022 3049 rBV 2268361 5297658 62.71% 12.015% 12 36.844 3456 3464 3490 rBV2 1547792 4217803 49.93% 9.566%

Sum of corrected areas: 44091364

9.D GCMS0208.M Fri Feb 08 13:44:25 2002

NYC-WTC_000050127

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NYC-WTC_000050127Source: NYC Law Department, mirrored locally

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