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GCMS sample results, AE00899, Feb 26, 2002

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Gas chromatography mass spectrometry results for sample AE00899 analyzed on February 26, 2002.

NYC-WTC_000009466–000009476

Folder label: “GCMS X 1/14/02 A 2/25-2/26

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\FEB1102\899.D Vial: 34 Acq On : 12 Feb 2002 8:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.221 341 346 354 rBV 11236 30971 1.48% 0.292% 2 12.342 790 795 807 rVB 612074 1633308 78.07% 15.410% 3 15.987 1186 1192 1204 rBV 985457 1979610 94.63% 18.678% 4 21.302 1765 1771 1779 rBV 1076933 2091987 100.00% 19.738% 5 25.755 2249 2256 2268 rBV2 997784 2053813 98.18% 19.378%

6 30.832 2804 2809 2814 rBV 168805 322246 15.40% 3.040% 7 33.824 3128 3135 3148 rBV 641392 1434490 68.57% 13.534% 8 36.294 3400 3404 3412 rBV2 20498 54895 2.62% 0.518% 9 38.112 3592 3602 3615 rBV2 325711 969985 46.37% 9.152% 10 47.898 4667 4668 4670 rVB 49731 27596 1.32% 0.260%

Sum of corrected areas: 10598901

899.D GCMS0208.M Wed Feb 20 09:53:02 2002

NYC-WTC_000009471

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NYC-WTC_000009471Source: NYC Law Department, mirrored locally

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