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GCMS analysis report for sample AE01040, Feb 2002

Machine-extracted title · confidence 50%

GC/MS analysis report for sample AE01040 showing surrogate recovery data generated on February 27, 2002.

NYC-WTC_000052759–000052769

Folder label: “GCMS X 1/15/02 A 2/11/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\FEB1102\1040.D Vial: 28 Acq On : 12 Feb-2002 12:27 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.251 126 132 141 rBV2 20597 46712 1.73% 0.338% 2 6.940 204 207 214 rBV 14811 31361 1.16% 0.227% 3 12.347 791 796 808 rVB 885639 1993556 73.69% 14.437% 4 15.992 1187 1193 1209 rBV 1286870 2520104 93.15% 18.251% 5 21.307 1766 1772 1782 rBV 1331265 2705431 100.00% 19.593%

6 25.759 2250 2257 2267 rBV 1288802 2692316 99.52% 19.498% 7 30.836 2805 2810 2815 rBV 200047 378435 13.99% 2.741% 8 33.829 3129 3136 3148 rBV 904499 2010785 74.32% 14.562% 9 36.445 3419 3421 3422 rBV 59132 33217 1.23% 0.241% 10 38.116 3594 3603 3618 rBV2 469078 1396300 51.61% 10.112%

Sum of corrected areas: 13808217

1040.D GCMS0208.M Tue Feb 19 10:33:34 2002

NYC-WTC_000052764

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NYC-WTC_000052764Source: NYC Law Department, mirrored locally

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