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GCMS analysis summary, sample AD31377, Feb 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31377 showing surrogate recovery and unknown compounds from February 7, 2002.

NYC-WTC_000016136–000016148

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31377.D Vial: 23 Acq On : 16 Jan 2002 8:28 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.446 258 262 297 rVB 308598 877008 15.93% 3.306% 2 11.495 699 703 722 rBV 1608331 4283264 77.82% 16.146% 3 15.093 1089 1095 1113 rBV 2584131 5371498 97.59% 20.248% 4 20.354 1662 1668 1689 rBV 2648597 5504303 100.00% 20.749% 5 24.769 2143 2149 2162 rBV2 2282888 4846673 88.05% 18.270%

6 29.846 2697 2702 2710 rBV 292566 579091 10.52% 2.183% 7 32.793 3017 3023 3038 rBV2 1160402 2736436 49.71% 10.315% 8 33.408 3085 3090 3102 rBV4 17155 56985 1.04% 0.215% 9 34.335 3185 3191 3199 rBV2 22261 73299 1.33% 0.276% 10 35.217 3282 3287 3299 rBV2 32812 128442 2.33% 0.484% 11 36.080 3374 3381 3389 rBV2 39096 143722 2.61% 0.542% 12 36.860 3460 3466 3475 rBV 713929 1927582 35.02% 7.266%

Sum of corrected areas: 26528303

31377.D GCMS1126.M Mon Feb 04 15:07:44 2002

NYC-WTC_000016141

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NYC-WTC_000016141Source: NYC Law Department, mirrored locally

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