GCMS sample AE11905 results, June 6 2002

NYC 9/11 Public Portal Document Llorary bearen compound keport

Data File C:\MSDCHEM\1\DATA\060402\11905.D Vial: 8 Acq On 4 Jun 2002 9:33 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 3-Amino-s-triazole Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 3.93 0.43 ug/L 291377 1,4-dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Amino-s-triazole 84 C2H4N4 000061-82-5 5/ 2 Dicyandiamide 84 C2H4N4 000461-58-5 4 3 2-Methyl[1,3,4]oxadiazole 84 C3H4N2O 003451-51-2 4 4 4H-l,2,4-Triazol-4-amine 84 C2H4N4 000584-13-4 4 Abundance Scan 145 (3.931 min): 11905.D (-144) (-) m/z 84.00 100 . 00% 84

47 51 5000

35 42 3.60 3.80 4.00 4.20 Oh -

.—mopss. I' “ • i “ " i “ “ i ‘ ■ i • ■ ■ ■ i ■1" i ■ ■ “ i “ “ i m/z 47.00 57.49% miz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116541:3-Amino-s-triazole 84

28 5000- ■ ■ i ■ ‘ • i ■ ■ ' ‘ i ■ ■ ■ ■ i ■ ■ ■ ■ i 57 3,60 3.80 4.00 4.20 43 m/z 51.10 51.40%

n/z-> Abundance Oj-r 15 -H ■ i'' ■ ■ i1 ■I "“I" Up 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

43 53 1 ■ i ■ ■ ■ • i ■ ■ ■ ■ i1 ■ ■ ■ i' ■ • ■ i ■ ■

#116556: Dicyandiamide 84 11" ■ ■ i /rsas. ■ ■ i ■ ■ ■ 1 i ■ ‘ ' ■ i ■ ‘ ■ ■ i ■ ■ ■ ' i 3.60 3.80 4.00 4.20 5000 68 m/z 85.00 18.36%

=4 56 Or 0 h11 ■'i" '■ 111111''1 ■ i■ 'i ■11 ' i ■ ■ ■ • i ■' ■ 111111111' । niz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33601:2-Methy[1,3,4]oxadiazole 84 3.60 3.80 4.00 4.20 ‘‘ 43 m/z 42.00 11.28% 5000 27 55 WaWWaluuytot n/z-> O- ■' I' IT’I I 15 20 25 20.— — 40 —++ 51 TTT+ 69 81 ’1 1 ■‘।i' " 11■ ■ ■ ■ i ■ “11' " 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20

11905.D 060302.M Wed Jun 05 14:03:48 2002 Page 10

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