GCMS blank analysis results, June 11 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\0610022\LB.D Vial: 7 Acq On : 10 Jun 2002 3:54 pm Operator: Sample : gc/ms scan 6/7 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params.: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L

Peak Number 8 3-Amino-s-triazole Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

4.04 2.28 ug/L 1704690 1,4-dichlorobenzene-d4 9.89

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Amino-s-triazole 84 C2H4N4 000061-82-5 7 2 4H-1,2,4-Triazol-4-amine 84 C2H4N4 000584-13-4/7 3 Pyridine-d5- 84 C5D5N 007291-22-7 7 4 Perdeuterobenzene 84 C6D6 001076-43-3 5 Abundance Scan 163 (4.037 min): LB.D (-161) (-) m/z. 49.10 100.00% 40 84

5000

42 152 i ■ 1 ■ ' i ‘ ■ i 1 ■ ■ ‘ i ■ ' 38 87 3.60 3.80 4.00 4.20 4.40 0!1’1-1111117’191211111111137 ——7103TTr "i■ ■ ■ i‘ "i“'■ i“i""i""i'■ “i'■1 m/z 84.00 94.22% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116542: 3-Amino-s-triazole 84 28 57 5000 i ' • ' ■ i • ■ ■ ' i ■ ' ■ ■ i ■ ' 3.60 3.80 4.00 4.20 4.40 43 m/z 51.05 65.46% 54 miz-> . I I I?. 491, -++ T-T 0+ ' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ 67_________ —gmmmgortt 5 W 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 •i ■"11 ■

Abundance #107976:4H-1,2,4-Triazol-4-amine 28 84 3.60 3.80 4.00 4.20 4.40 5000 m/z .42.00 21.32%

18 42 69 53 57 miz-> O+ ........ 4.2% 21.3639,145.. 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 TTTTTTTTTT Tmmp Abundance #33686: Pyridine-d5- 56 84 3.60 3.80 4.00 4.20 4.40 m/z 52.10 18.42% 5000 52 28 38 42

n/z-> 0 14 24] I I | > I I I | ) 1 l t | ITI [ | l 1 t t J i i !i 32—4411.48—4. , 62 66 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 76 I H | I 1 1 I | 1 I nmr 1 I | I I 1 1 | ! — 3.60 3.80 4.00 ! 4.20 4.40

LB.D 060302.M Tue Jun 11 08:25:48 2002 Page 11

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