GCMS sample AE12765 results, June 6 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\060402\12765.D Vial: 6 Acq On 4 Jun 2002 7:55 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 1 1-Propanethiol Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T.

3.53 0.40 ug/L 254916 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qua!

1 1-Propanethiol 76 C3H8S 000107-03-9 7 2 Propanoic acid 74 C3H602 000079-09-4/5 3 Carbonic chloride fluoride 82 CC1FO 000353-49-1 4 4 Acetonitrile, dichloro-_________________ :109 C2HC12N 003018-12-0 4 Abundance Scan 76 (3.526 min): 12765.D (-73) (-) m/z 74.00 00.00% 74 82 47 5000

50 54 88 35. 37 | 40 3.20 3.40 3.60 3.80 II.]... mm

A Of "i tmrpu " p ■ ■■ i ■■ ■ ■ !■■ ■ ■ i ■ ■ ■ । j ■ ■ ■ ■ i H1 ■ b i1 m/z 81.95 72.70% mz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #111007:1 -Propanethiol 43 47 27 76

5000 39 3.20 3.40 3.60 3,80 m/z 47.10 65.95%

miz-> 0!

Abundance 15

5 10 15 20 241120,18all 12, TTTTHTT TT 33 iff.. Al... ,69,73 +9- 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #115380: Propanoic acid 45 F661

74 u/y 3.20 3.40 3.60 3.80 5000 m/z 84.00 .65.47% 57

n/z-> ol 5 36 42 TH+ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 49 ■ i"' ■ i' ■ 84 88 " i •'111 •41 ■ i1" * i * •

Abundance #12296: Carbonic chloride fluoride 47 3.20 3.40 3.60 3.80 m/z 75.95 38.77%

5000 82 44 ............................. ................... 28 35 63 12 18 | 31 38 54 60 | 66 77 85 0 T‘ i “ ■ ■ i ■' ■ ■ i"1 ‘ i ■■ “ i ■ ■ ।' i11' ■ 't' i ■" T’ + । > rp 11 > 111111111. p-i ■■■> I', Prir T| >: 111111 ’I’T miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.20 3.40 3.60 3.80

12765.D 060302.M Wed Jun 05 14:05:15 2002 Page 4

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