GCMS analysis results, sample AE12325, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052902\12325 .D Vial: 13 Acq On : 29 May 2002 7:51 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 1 1-Propanethiol Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 3.54 0.22 ug/L 155092 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qua 1 1-Propanethiol 76 C3H8S 000107-03-9 22 2 1-Propanethiol 76 C3H8S 000107-03-9 22 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12/0 9 4 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 9 Abundance Scan 79 (3.543 min): 12325.D (-73) (-) m/z 74.00 100.00% 74 47 82 5000

36 88 ... M 3.20 3.40 3.60 3.80 Of . 10........... Mln + ............ I m/z 47.10 50.97%

"uhaa/Mnp ■ i ■ ■ ■ ■ i ■ TIB 1 i ‘ ■ i ■ ■ ■ ■ i ■ ■ ■ ' । miz-> 20 30 40 50 60 70 80 90 100 110 Abundance #111021:1-Propanethiol 47 76 41 27 5000 3.20 3.40 3.60 3.80 61 m/z 82.00 49.03% 15 35

Tl/Z-> Abundance ol

5000 — 10 L —ull + 15541., 69 20 30 40 50 60 70

27 41 #111007:1-Propanethiol 47 76 'I । 80 । 90 j .... j .... ( 100 110

nA//MAA j .MMwnmrw 3.20 m/Z .L 3.40 3.60 76.00 3.80 39.56%

m/z-> 01 15 ■ ■ ■ l „I 10 20 +l + —R— 30 40 50 60 61

70 80 'I । 90 । ( 100 j . । 110 j

Abundance #28338: Acetonitrile, dichloro- 1 1" ‘ 1‘ • ■ । ' i 1 74 3.20 3.40 3.60 3.80 m/ z 84.00 22.22% 5000 82 47 35

/z-> 0 12 26 I i[l , 1111 • ■ ■ ।1 111 1 1 1 1 1 1 ' 10 20। 30 40 +-50—602— 70 80 , 108 ' 1 1111* 111 1 1 1 i 90 100 110 TIB ■ । 3.20 ‘ । ■ ■ ■ ■ । 1 ■ 1 1 i' 1 1 1 i1 3.40 3.60 3.80

12325.D 052202.M Mon Jun 03 10:53:19 2002 Page 4

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