GCMS sample AE12762 results, June 10 2002

NYC 9/11 Public Portal Document Llorary searcr compound Keporc Data File C:\MSDCHEM\l\DATA\060702\12764.D Vial: 4 Acq On 7 Jun 2002 11:02 am Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 13 2-Chloro-4-aminopyrimidine Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.

5.00 1.40 ug/L 835092 1,4-dichlorobenzene-d4 9.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Chloro-4-aminopyrimidine 129 C4H4C1N3 007461-50-9 2 2,4-Dicyanopyridine 129 C7H3N3 029181-50-8 4 3 Pyridine, 2-chloro-4-methyl- 127 C6H6C1N 003678-62 4 4 4 o-Chloroaniline 127 C6H6C1N 000095-5 -2 4 Abundance Scan 328 (5.006 min): 12764.D (-324) (-) m/z 128.85 /100.00%

.h 129

49 5000 88

208

niz-> 0- —L. 20 37 ,

40 ’ I ‘ 60 70 80 ' T' 1...I . 100 120 140 160 180 200 4.60 m/z 126.85 4.80 5.00 5.20 5.40 89.12% Abundance #58331:2-Chloro-4-aminopyrimidine 129

5000 28 41 67 94 .... M... 4.60 m/z 4.80 49.10 5.00 5.20 5.40 57.79%

iz-> 0- i ,il 52 -ll-+ll———L+177 20 40 60 80 —L 100 104 116 T 120 140 160 180 200 Abundance #58357:2,4-Dicyanopyridine 129 ■ i 1 ‘ ■ i ■ 1 4.60 4.80 5.00 5.20 5.40 5000- m/ z 51.05 53.52% 51 102 75 26 38 62 89

niz-> 12 0- ■i । *r । Ji । Il 20 40 । rh ill 60 18 80 -l— 100 120 140 l 160 180 200 Abundance #57621: Pyridine, 2-chloro-4-methyl- 92 127 4.60 4.80 5.00 5.20 5.40 m/z 130.90 41.51% 5000 65

39 . 51 , 0 . jm il J, , 78 ‘I ‘ 11 m/z-> 20 40 60 80 100 120 140 160 180 200 4.60 4.80 5.00 5.20 5.40

12764.D 060302.M Mon Jun 10 10:30:04 2002 Page 16

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