GCMS sample AE12762 results, June 10 2002

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Data File C:\MSDCHEM\l\DATA\060702\12764.D Vial: 4 Acq On 7 Jun 2002 11:02 am Operator: Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan ’5 Library : C: \DATABASE\NIST98 . L

Peak Number 14 4H-l,2,4-Triazol-4-amine Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T.

5.26 0.26 ug/L 154273 1,4-dichlorobenzene-d4 9.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4H-1,2,4-Triazol-4-amine 84 C2H4N4 000584-13-4 10 2 4H-1,2,4-Triazol-4-amine 84 C2H4N4 000584-13-4 9 3 Thiophene 84 C4H4S 000110-02-1/5 4 Dicyandiamide 84 C2H4N4 000461-58-5 5 Abundance Scan 371 (5.259 min): 12764.D (-370) (-) m/z 86.00 0.00% 85

5000 49 70 5.00 5.20 5.40 5.60 Ot 40,44 TTTTTTTTTTTTTTT 82 m/z 84.00 96.87% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 I'''' I■''' I ■" 'I ■ ■

Abundance #33490:4H-1,2,4-Triazol-4-amine 28 84

5000 5.00 5.20 5.40 5.60 m/z 49.10 36.33% 13 18 32 4043 57 69

miz—> 0! 5 -H 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 35 ■ ■ “ i ■ ■" i ■

Abundance #107976:4H-1,2,4-Triazol-4-amine 28 84 5.00 5.20 5.40 5.60 5000 m/z 51.10 23.21%

18 42 31 3639 53 5768 1/45 iz-> 0! .5.. 101111/111.11.25 ftTl l I l I II I | ■ I Tyanu ‘ 4+11-11-4-1+***14*--1*2**1****1‘4* 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116585: Thiophene 84 5.00 5.20 5.40 5.60 m/z 70.00 16.65% 58 5000 45 39

m/z-> 12 18 26 32 36, 42 o 1 I r. ... | . I I ! | .... | .... | I I , , ! 50 „9,1176.81/ 7 ( 61 I | | I , 1 1 1 . I | I ! . , | I I Hmm TII 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 5.00 5.20 5.40 5.60

12764.D 060302.M Mon Jun 10 10:30:05 2002 Page 17

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