GCMS calibration report for sample AE12224, June 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JUNO302\CALIO.D Vial: 2 Acq On 3 Jun 2002 9:41 am Operator: Morgan Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 11:43 2002 Quant Results File: -GCMS0531 .RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 474420 40.00 ug/1 0.00 10) Naphthalene-d8 15.70 136 1894469 40.00 ug/1 -0.02 17) Acenaphthene-diO 20.99 164 893048 40.00 ug/1 0.00 3 0) Phenanthrene-dl0 25.43 188 1397890 40.00 ug/1 0.00 38) Chrysene-dl2 33.48 240 879789 40.00 ug/1 -0.03 44) Perylene-dl2 37.65 264 550271 40.00 ug/1 -0.03 System Monitoring Compounds 28) TCMX 23.14 209 242947 39.32 ug/L 0.00 Spiked Amount 40.000 Recovery 98.30% Target Compounds 2) N-nitrosodimethylamine 5.73 74 120098 7(7 ug/1 8.27 Qvalue 98 3) bis(2-Chloroethyl)ether 11.47 93 161840 8.53 ug/1 98 4) 1,3-Dichlorobenzene 11.97 146 164173 8.71 ug/1 97 5) 1,4-Dichlorobenzene 12.12 146 182561 8.94 ug/1 100 6) 1,2-Dichlorobenzene 12.63 146 158472 8.82 ug/1 99 7) 2,2’-oxybis(1-Chloropropan 12.95 45 252351 8.51 ug/1 99 8) N-Nitrosodi-n-propylamine 13.34 70 108768 8.29 ug/1 99 9) Hexachloroethane 13.47 117 71927 8.92 ug/1 98 11) Nitrobenzene 13.75 77 146557 8.38 ug/1 97 12) Isophorone 14.39 82 277176 8.45 ug/1 100 13) bis(2-Chloroethoxy)methane 15.08 93 185003 8.58 ug/1 99 14) 1,2,4-Trichlorobenzene 15.59 180 132770 9.04 ug/1 98 15) Naphthalene 15.75 128 456024 9.15 ug/1 99 16) Hexachlorobutadiene 16.30 225 57466 8.89 ug/1 97 18) Hexachlorocyclopentadiene 18.50 237 40172 7.33 ug/1 98 19) 2-Chioronaphthalene 19.25 162 213561 8.98 ug/1 99 20) Dimethylphthalate 20.35 163 267317 8.84 ug/1 99 21) 2,6-Dinitrotoluene 20.56 165 52621 7.71 ug/1 97 2 2) Acenaphthylene 20.52 152 384630 9.01 ug/1 99 2 3) Acenaphthene 21.08 153 239965 9.34 ug/1 99 24) 2,4-Dinitrotoluene 21.73 165 56006 7.01 ug/1 97 25) Diethylphthalate 22.48 149 246838 8.82 ug/1 100 26) 4-Chlorophenylphenylether 22.63 204 127966 9.61 ug/1 97 27) Fluorene 22.60 166 254195 9.74 ug/1 99 29) Azobenzene 23.09 77 297546 8.60 ug/L 97 31) N-Nitrosodiphenylamine 23.02 168 105827 10.37 ug/1 99 32) 4-Bromophenylphenylether 24.10 248 63259 9.02 ug/1 98 33) Hexachlorobenzene 24.53 284 72117 9.39 ug/1 96 34) Phenanthrene 25.49 178 376974 9.59 ug/1 99 (#) = qualifier out of range (m) = manual integration CAL10.D GCMS0531.M Mon Jun 03 14:27:49 2002 Page 1

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