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GCMS sample results AE12096, DEP Labs, June 2002

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Gas chromatography mass spectrometry results for sample AE12096 analyzed on June 4, 2002.

NYC-WTC_000014836–000014842

Folder label: “GCMS X 5/29/02 A 5/30/02

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NYC 9/11 Public Portal Document 6 Quantitation. Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2302\12096.D Vial: 11 Acq On : 23 May 2002 9:59 pm Operator: Morgan Sample : 5/21 bn Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 31 15:48 2002 Quant Results File:„GCM60520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) . y A Title : 209 625/TCLP calibration table U • p) Last Update : Fri May 31 15:47:14 2002 oD A/ Response via : Initial Calibration V ) • PMA DataAcq Meth : GCMS0520 WN / V 0

Internal Standards R.T. Qlon Response Cone Units Dev (Min) 1) l,4-Dichlorobenzene-d4 12.14 152 485854 40.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 1764616 40.00 ug/1 0.00 17) Acenaphthene-diO 21.08 164 954913 40.00 ug/1 0.00 30) Phenanthrene-diO 25.52 188 1266826 40.00 ug/1 -0.01 38) Chrysene-dl2 33.57 240 741631 40.00 ug/1 -0.03 44) Perylene-dl2 37.79 264 508144 40.00 uq/I -0.02

System Monitoring Compounds 28) TCMX 23.23 209 132545 :27.62 Jug/L 0.00 Spiked Amount 40.000 Recovery• = < 69. 69.05% Target Compounds Qvaluj 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.57 149 242 N.D. 26) 4-Chlorophenylphehylether 23.23 204 443 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.22 168 368 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.52 178 226 N.D. (#) = qualifier out of range (m) = manual integration 12096.D GCMS0520.M Fri May 31 15:49:28 2002 Page 1

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