GCMS calibration data AE11284, DEP Labs, May 2002

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Calibration data for sample AE11284 analyzed using Method 508 on May 17, 2002.

NYC-WTC_000014807–000014817

Folder label: “GCMS X 5/29/02 A 5/30/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAY3002\12095.D Vial: 14 Acq On : 31 May 2002 2:51 am Operator: Morgan Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 31 11:26 2002 Quant Results 1500 Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.06 152 558543 40.00 ug/1 -0.08 10) Naphthalene-d8 15.69 136 2251912 40.00 ug/1 -0.10 17) Acenaphthene-diO 20.99 164 1072566 40.00 ug/1 -0.10 30) Phenanthrene-diO 25.43 188 1649713 40.00 ug/1 -0.10 38) Chrysene-dl2 33.47 240 1001566 40.00 ug/1 -0.13 44) Perylene-dl2 37.66 264 634901 40.00 ug/1 -0.14

System Monitoring Compounds 28) TCMX 23.14 209 187738 34.83 ug/L -0.10 Spiked Amount 40.000 Recovery 87.07% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.37 74 544 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.07 146 485 N.D. 5) 1,4-Dichlorobenzene 12.07 146 485 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.75 128 210 N.D. 16) Hexachlorobut adi ene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.28 165 378 N.D. 25) Diethylphthalate 22.48 149 1668 N.D. 26) 4-Chlorophenylphenylether 23.14 204 958 N.D. 2 7) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.13 168 419 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.43 178 642 N.D. (#) = qualifier out of range (m) = manual integration 12095.D GCMS0520.M Fri May 31 11:26:23 2002 Page 1

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GCMS calibration data AE12095, DEP Labs, May 2002 · Box DEP Box 15

NYC-WTC_000014825

Calibration table and internal standard data for sample AE12095 analyzed on May 31, 2002.

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