Gas chromatography-mass spectrometry analysis of sample AE12223 conducted on June 3, 2002, detecting unknown compounds and 2,4-DDD surrogate at 76% recovery.
NYC-WTC_000013864–000013872Folder label: “GCMS X 5/23/02 A 5/29/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\MAY2902\12223.D Vial: 13 Acq On : 29 May 2002 11:08 pm Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 30 8:28 2002 Quant Results File: GCMS0528.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 08:55:48 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1, 4-Dichlorobenzene-d4 12.07 152 535529 40.00 ug/1 -0.07 10) Naphthalene-d8 15.70 136 2151519 40.00 ug/1 -0.09 17) Acenaphthene-diO 21.00 164 1031236 40.00 ug/1 -0.09 30) Phenanthrene-diO 25.43 188 1550181 40.00 ug/1 -0.10 38) Chrysene-dl2 33.47 240 889074 40.00 ug/1 -0.14 44) Perylene-dl2 37.66 264 564588 40.00 ug/1 -0.15
System Monitoring Compounds 28) TCMX 23.13 209 217275 30.52 ug/L -0.10 Spiked Amount 40.000 Recovery 76.30% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.34 74 207 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.05 146 521 N.D. 5) 1,4-Dichlorobenzene 12.05 146 521 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.31 77 170 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.75 128 614 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.35 163 215 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.48 149 1543 N.D. 26) 4-Chlorophenylphenylether 23.13 204 1552 N.D. 27) Fluorene 0.00 166 0 N.D. 2 9) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.13 168 692 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 3 3) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.49 178 1245 N.D. (#) = qualifier out of range (m) = manual integration 12223.D GCMS0528.M Thu May 30 08:28:52 2002 Page 1
NYC-WTC_000013866
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NYC-WTC_000013873
GCMS analysis results for sample AE12225 dated June 3, 2002, documenting unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013834
GCMS analysis results for sample AE12168 dated June 3, 2002, documenting unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013825
GCMS analysis results for sample AE12166 dated June 3, 2002, documenting unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013816
GCMS analysis results for sample AE12165 dated June 3, 2002, documenting unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013342
Analytical report for sample AE12153 detailing GCMS results and surrogate recovery data from June 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014934
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12577 conducted on June 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013351
Analytical report for sample AE12154 detailing GCMS results and surrogate recovery data from June 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013378
Gas chromatography-mass spectrometry analysis of sample AE12157 performed on 6/7/02, detecting unknown compounds and 2,4-DDD surrogate at 83% recovery.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013387
Laboratory report documenting GCMS analysis of sample AE12158 conducted on June 7, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013396
Laboratory report documenting GCMS analysis of sample AE12159 conducted on June 7, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013360
Analytical report for sample AE12155 detailing GCMS results and surrogate recovery data from June 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013843
GCMS analysis results for sample AE12169 dated June 3, 2002, documenting unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000013772
DEP document containing gas chromatography-mass spectrometry data from late May 2002.
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NYC-WTC_000013773
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NYC-WTC_000013775
Laboratory report documenting GCMS analysis of sample AE12163 conducted on May 29, 2002.
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NYC-WTC_000013783
Laboratory blank analysis report for volatile organic compounds including nitrosamines and chlorinated benzenes dated May 29, 2002.
Filed in the same folder
NYC-WTC_000013787
Calibration results for GCMS analysis of volatile organic compounds including nitrosamines and chlorinated benzenes.
Filed in the same folder