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GCMS analysis results, sample AE12223, June 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AE12223 conducted on June 3, 2002, detecting unknown compounds and 2,4-DDD surrogate at 76% recovery.

NYC-WTC_000013864–000013872

Folder label: “GCMS X 5/23/02 A 5/29/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\MAY2902\12223.D Vial: 13 Acq On : 29 May 2002 11:08 pm Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 30 8:28 2002 Quant Results File: GCMS0528.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 08:55:48 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.63 178 293 N.D. 36) Di-n-butylphthalate 27.41 149 33782 0.66 ug/1 100 37) Fluoranthene 29.11 202 2017 N.D. 39) Pyrene 29.79 202 2019 N.D. 40) Butylbenzylphthalate 31.93 149 712 N.D. 41) Benzo(a)anthracene 33.47 228 2091 N.D. 42) Bis(2-ethylhexyl)phthalate 33.71 149 7823 0.36 ug/1 99 43) Chrysene 33.54 228 286 N.D. 45) Di-n-Octylphthalate 35.47 149 263 N.D. 46) Benzo(b)fluoranthene 36.52 252 213 N.D. 47) Benzo(k)fluoranthene 36.57 252 243 N.D. 4 8) Benzo(a)pyrene 37.48 252 212 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 12223.D GCMS0528.M Thu May 30 08:28:53 2002 Page 2

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