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← Document results/DEP Box 15/GCMS X 5/23/02 A 5/29/02
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GCMS unknowns report, DEP Box 15, June 2002

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GCMS analysis results for sample AE12165 dated June 3, 2002, documenting unknown compounds and surrogate recovery.

NYC-WTC_000013816–000013824

Folder label: “GCMS X 5/23/02 A 5/29/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY2902\12165.D Vial: 8 Acq On : 29 May 2002 6:13 pm Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 30 8:21 2002 Quant Results File:GCMS0528.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 08:55:48 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Compound R.T. Qlon Response Cone Unit Qvalue 3 5) Anthracene 25.50 178 500 N.D. 36) Di-n-butylphthalate 27.41 149 35904 0.62 ug/1 98 3 7) Fluoranthene 29.11 202 346 N.D. 39) Pyrene 29.78 202 472 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.47 228 2900 N.D. 42) Bis(2-ethylhexyl)phthalate 33.70 149 1895 N.D. 43) Chrysene 33.54 228 658 N.D. 45) Di-n-Octylphthalate 35.45 149 538 N.D. 46) Benzo(b)fluoranthene 36.52 252 957 N.D. 47) Benzo(k)fluoranthene 36.58 252 1676 N.D. 48) Benzo(a)pyrene 37.48 252 846 N.D. 49) Indeno(1,2,3-cd)pyrene 41.64 276 275 N.D. 50) Dibenz(a,h)anthracene 41.72 278 272 N.D. 51) Benzo(g,h,i)perylene 42.82 276 754 N.D.

(#) = qualifier out of range (m) = manual integration ‘ 12165.D GCMS0528.M Thu May 30 08:22:07 2002 Page 2

NYC-WTC_000013819

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NYC-WTC_000013819Source: NYC Law Department, mirrored locally

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