GCMS unknowns report for sample AE12284, June 2002

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Report documenting analysis for unknown compounds and surrogate recovery in sample AE12284.

NYC-WTC_000013762–000013771

Folder label: “GCMS X 5/23/02 A 5/30/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\MAY2902\12284.D Vial: 24 Acq On : 30 May 2002 9:55 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 30 11:09 2002 Quant Results File: GCMS0528.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 08:55:48 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 575207 40.00 ug/1 -0.08 10) Naphthalene-d8 15.69 136 2291786 40.00 ug/1 -0.10 17) Acenaphthene-diO 20.99 164 1104666 40.00 ug/1 -0.10 3 0) Phenanthrene-dl0 25.42 188 1722572 40.00 ug/1 -0.11 38) Chrysene-dl2 33.47 240 1045639 40.00 ug/1 -0.13 44) Perylene-dl2 37.65 264 677880 40.00 ug/1 -0.15 System Monitoring Compounds 28) TCMX 23.13 209 220168 28.87 ug/L -0.11 Spiked Amount 40.000 Recovery 72.18% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.06 146 377 N.D. 5) 1,4-Dichlorobenzene 12.06 146 377 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.89 77 102 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.30 165 195 N.D. 25) Diethylphthalate 22.48 149 1223 N.D. 26) 4-Chlorophenylphenylether 23.13 204 1454 N.D. 27) Fluorene 0.00 166 0 N.D. 2 9) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.13 168 687 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.41 178 840 N.D. (#) = qualifier out of range (m) = manual integration 12284.D GCMS0528.M Thu May 30 11:09:40 2002 Page 1

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