GCMS analysis results, sample AE12534, June 2002

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Laboratory report showing GCMS analysis results for sample AE12534 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014578–000014606

Folder label: “GCMS X 5/28/02 A 5/29/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052902\12534.D Vial: 25 Acq On : 30 May 2002 5:37 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ******************************************************* * * ************ Peak Number 16 Phenyl t-butyl telluride Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

34.91 0.34 ug/L ’ 149443 Perylene-dl2 34.65

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phenyl t-butyl telluride 264 C10H14Te 1000148-36-6 2 2 Isobenzofuran-1,3-dione, 4,5-dim. .. 208 C10H8O5 001567-56-2 12 3 1H-Indole, 3-methyl-2-(2’-pyridyl)- 208 C14H12N2 000951-25-77* 4 Dibenzo[b,E]-1,4-diazabicyclo[2 .... 208 C14H12N2 094509-68-9 7 Abundance Scan 5417 (34,907 min): 12534.D (-5415) (-) m/z 265.10 100.00% 96 208 205 131 5000 49 84

34.60 34.80 35.00 35.20 0! 1 m/z 264.10 95.26% niz-> :20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #95144: Phenyl t-butyl telluride 2614

208 - 5000 78 34.60 34.80 35.00 35.20 130 m/z 96.00 94.83% 91 155167179 1 01 I ‘ ‘ ’ I ‘ 1 ‘ ‘ ‘ ‘ I *‘*•1***1* • t ■ ■ ■ 1 i ' ' ■ • i 1 ■ ■ 1 i •‘ I * 1 • ‘TT' m/z-> Abundance> :20 40 60 80 100 120 140 160 180 200 220 240 260 #84979: Isobenzofuran-1,3-dione, 4,5-dimethoxy- A 78 208 44 104 . II. 11 ‘ ‘ I ‘ 1 ‘ ‘ I ‘ ‘ f-r-r 135 34.60 34.80 35.00 35.20 5000 m/z 262.10 92.67% 65 163 179 122 150 I ill Li 1. 193 193 miz—> 0- I 1 ■ ■ ■ iIIT 20 40 60 80 -hl— hi r ..... 100 120 140 160 180 200 220 240 260 Abundance #85111:1 H-Indole, 3-methyl-2-(2-pyridy!)- 208 34,60 34.80 35.00 35.20 m/z 207.90 80.60%

5000

130

n/z-> 0 27,39,51,63,790/72117. 20 40 152 167180192 1 60 80 100 120 140 160 180 200 220 240 260 ■ 1 ■ ■ i l " ' " ■' t r l " • j • ■ - ■ i • • ■ * i ■ * wiw/ Wrwrone diAina 34.60 34.80 35.00 35.20

12534.D 052202.M Mon Jun 03 11:46:54 2002 Page 19

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