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GCMS calibration results for VOCs, sample AE12326, June 2002

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Laboratory report showing GCMS calibration data for volatile organic compounds in sample AE12326 on June 3, 2002.

NYC-WTC_000014375–000014378

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document quanttaton Report (QT Reviewed) Data File C:\MSDCHEM\l\DATA\052902\CAL80.D Vial: 2 Acq On 29 May 2002 10:54 am Operator: McLean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 04 11:56:57 2002 Quant Results File: 052202.RES Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Tue Jun 04 11:56:53 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoroanthene 26.52 202 35193828 72.65 ug/L 99 3 8) Pyrene 27.15 202 33815281 82.68 ug/L 99 39) Butylbenzylphthalate 29.49 149 14789891 84.50 ug/L 97 4 0) Benzo(a)anthracene 30.75 228 26722224 86.56 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.35 149 18486519 81.22 ug/L 97 42) Chrysene 30.86 228 26626691m 75.06 ug/L 44) Di-n-octylphthalate 33.20 149 27256646 95.87 ug/L 99 45) Benzo(b)fluoranthene 33.72 252 22237658 84.92 ug/L 99 46) Benzo(k)fluoranthene 33.80 252 24637061 83.99 ug/L 99 47) Benzo(a)pyrene 34.53 252 20994426 89.63 ug/L 99 48) Indeno(l,2,3-cd)pyrene 37.35 276 14186339 90.85 ug/L 97 49) Dibenz(a,h)anthracene 37.47 278 15177808 88.37 ug/L 99 50) Benzo(g,h,i)perylene 38.10 276 15790776 86.59 ug/L 97

(#) = qualifier out of range (m) = manual integration (+) signals summed CAL80.D 052202.M Tue Jun 04 11:58:56 2002 Page 2

NYC-WTC_000014377

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NYC-WTC_000014377Source: NYC Law Department, mirrored locally

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