TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
NYC-WTC_000013997–000014003Folder label: “GCMS X 5/24/02 A 5/28/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) 4 Data File : C:\HPCHEM\1\DATA\MAY2102\11603.D Vial: 32 Acq On : 22 May 2002 9:06 pm Operator: Sample : EXTRACT5/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 24 8:21 2002 Quant Results File: GCMS0520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.15 152 386307 40.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 1513198 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.09 164 731720 40.00 ug/1 0.00 30) Phenanthrene-diO 25.53 188 946172 40.00 ug/1 0.00 38) Chrysene-dl2 33.57 240 510271 40.00 ug/1 -0.04 44) Perylene-dl2 37.79 264 328173 40.00 ug/1 -0.02 System Monitoring Compounds 28) TCMX 23.23 209 137368 37.35 ug/L 0.00 Spiked Amount 40.000 Recovery 93.38% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 11.41 93 2785 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 14.49 82 1428 N.D. 13) bis(2-Chloroethoxy)methane 15.17 93 779 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.83 128 661 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 19.36 162 532 N.D. 20) Dimethylphthalate 20.44 163 2462 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 20.62 152 459 N.D. 2 3) Acenaphthene 21.17 153 768 N.D. 24) 2,4-Dinitrotoluene 21.83 165 346 N.D. 25) Diethylphthalate 22.57 149 10347 0.55 ug/1 98 26) 4-Chlorophenylphenylether 22.72 204 760 N.D. 27) Fluorene 22.70 166 1116 N.D. 2 9) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. d 32) 4-Bromophenylphenylether 24.19 248 596 N.D. 3 3) Hexachlorobenzene 24.62 284 402 N.D. 3 4) Phenanthrene 25.59 178 4860 N.D. (#) = qualifier out of range (m) = manual integration 11603.D GCMS0520.M Fri May 24 08:21:56 2002 Page 1
NYC-WTC_000013997
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NYC-WTC_000013251
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013217
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013146
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013184
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023701
Laboratory report of GCMS analysis for sample AE10063 conducted on May 23, 2002, showing surrogate recovery data.
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Laboratory report of GCMS analysis for sample AE09680 conducted on May 23, 2002, showing surrogate recovery data.
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Laboratory report of GCMS analysis for sample AE10062 conducted on May 23, 2002, showing surrogate recovery data.
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Laboratory report of GCMS analysis for sample AE09654 conducted on May 23, 2002, showing surrogate recovery data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022902
Reviewed data file listing retention times and response factors for deuterated internal standards.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023811
Laboratory report of GCMS analysis for sample AE09676 conducted on May 23, 2002, showing surrogate recovery data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023738
Laboratory report of GCMS analysis for sample AE10065 conducted on May 23, 2002, showing surrogate recovery data.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043482
Gas chromatography-mass spectrometry analysis report for sample AE07107 including surrogate compound recovery data.
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NYC-WTC_000022670
Laboratory record of analytical results for environmental sample AE11795 with surrogate recovery information.
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Report detailing analytical findings for environmental sample AE11794 including surrogate compound data.
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Report documenting the identification of other unknown compounds and surrogate recovery for sample AE11604.
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Laboratory report presenting analytical data for environmental sample AE11797 and surrogate recovery metrics.
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Data sheet documenting GCMS analysis of environmental sample AE11796 and associated surrogate compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022698
Laboratory report presenting analytical data for environmental sample AE11798 and surrogate recovery metrics.
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NYC-WTC_000013882
Department of Environmental Protection record of GCMS results generated in late May 2002.
Filed in the same folder
NYC-WTC_000013883
Fragmented document header from DEP Box 15 archive containing metadata for environmental testing records dated late May 2002.
Filed in the same folder
NYC-WTC_000013909
GCMS calibration report for sample AE11602 dated May 30, 2002, showing quantitative results for volatile organic compounds.
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NYC-WTC_000013913
GCMS calculation report for sample AE11602 dated May 30, 2002, listing concentrations of nitrosamines and chlorinated compounds.
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NYC-WTC_000013921
GCMS analysis report for sample AE11602 dated June 4, 2002, documenting unknown compounds and surrogate recovery.
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