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GCMS analysis results, sample AE11796, May 2002

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Data sheet documenting GCMS analysis of environmental sample AE11796 and associated surrogate compounds.

NYC-WTC_000022679–000022687

Folder label: “GCMS X 5/20/02 A 5/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2102\11796.D Vial: 37 Acq On : 23 May 2002 2:04 am Operator: Sample : EXTRACT5/20 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 24 8:27 2002 Quant Results File: GCMS0520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.14 152 388042 40.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 1526818 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.09 164 732699 40.00 ug/1 0.00 30) Phenanthrene-di O 25.53 188 952988 40.00 ug/1 0.00 38) Chrysene-dl2 33.60 240 531787 40.00 ug/1 0.00 44) Perylene-dl2 37.82 264 338343 40.00 ug/1 0.02 System Monitoring Compounds 2 8) TCMX 23.23 209 136262 37.00 ug/L 0.00 Spiked Amount 40.000 Recovery 92.50% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.82 128 326 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Ac enapht hene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.58 149 688 N.D. 26) 4-Chlorophenylphenylether 23.23 204 584 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.23 168 430 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.53 178 191 N.D. (#) = qualifier out of range (m) = manual integration 11796.D GCMS0520.M Fri May 24 08:27:30 2002 Page 1

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