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← Document results/DEP Box 15/GCMS X 5/24/02 A 5/28/02
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GCMS analysis results for sample AE11603, June 2002

Machine-extracted title · confidence 90%

TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.

NYC-WTC_000013997–000014003

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY2102\11603.D Vial: 32 Acq On : 22 May 2002 9:06 pm Operator: Sample : EXTRACT5/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 24 8:21 2002 Quant Results File:,GCMS0520 .RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Compound R.T. Qlon Response Cone Unit Qvalue

35) Anthracene 25.59 178 4859 N.D. 36) Di-n-butylphthalate 27.50 149 41042 1.32 ug/1 99 3 7) Fluoranthene 29.21 202 7256 0.31 ug/1 97 3 9) Pyrene 29.89 202 6428 0.34 ug/1 # 92 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.58 228 1589 N.D. 42) Bis(2-ethylhexyl)phthalate 33.80 149 1704 N.D. 43) Chrysene 33.65 228 685 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.79 252 1273 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 11603.D GCMS0520.M Fri May 24 08:21:57 2002 Page 2

NYC-WTC_000013998

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NYC-WTC_000013998Source: NYC Law Department, mirrored locally

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