GCMS calculation results for sample AE11602, May 2002

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GCMS analysis report for sample AE11602 dated June 4, 2002, documenting unknown compounds and surrogate recovery.

NYC-WTC_000013921–000013942

Folder label: “GCMS X 5/24/02 A 5/28/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052802\11602.D Vial: 8 Acq On : 28 May 2002 8:00 pm Operator: McLean Sample : 5/24 ad re-ext Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 9 N-(2-Acetylcyclopentylidene... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 5.36 0.24 ug/L 159542 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-(2-Acetylcyclopentylidene)cycl... 207 C13H21NO 1000100-48-5 9 2 5-Methyl-2-phenylindolizine 207 C15H13N 036944-99-7 5 3 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4/5 4 2-Imidazolidinone 86 C3H6N20 000120-93-/4 5 Abundance Scan 389 (5.365 min): 11602.D (-386) (-) m/z 207.00 100.00% 207

5000 86 41 96 500 5.20 5.40 5.60 5.80

nfe-> 0: -rpf 58 L mH rrp-r Tp-rTTYTTTTp-rrrpTT-rpT-rrp-rfTp-rTTp-^^ 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 -p-TTT m/z 86.00 42.97% Abundance #84801: N-(2-Acetylcyclopentylidene)cyclohexylamine 207 164 124 41 5000 55 500 5.20 5.40 5.60 5.80 67 82 97 110 150 m/z 41.00 30.17% 192 136 178

niz-> 0 1117 Tp-rt-rpT-rr ““i' 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 “i” 1’183 H Abundance #84865:5-Methyl-2-phenylindolizine 207

5.00 5.20 5.40 5.60 5.80 5000 m/z 96.20 21,14%

28 39 51 63 77 89 102 115 130139 152 165 178 191 0 11 ■ 11'1'1111 rrr i ■ rri I d’r’r I1!1! jl'l r’rrrer’hre | r’ri prrrl 11 i’m i i rh 11 Mrrpi’ 11 r-i . i [T ■piTT nfe-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #84862: Pyrido[2,3-d]pyrimidine, 4-phenyl- _____________________________ 1 1 i ■ ■ ■ ■ i ' ■ ■ •! *’’I’+II 207 500 5.20 5.40 5.60 5.80 m/z 207.95 19.09% 5000 179 77 i — 103 127 152 0 . ।.... (., j “ 111) I,. । ।,i .11 11 >87 1'11111 I 111 n i > 11 rHn'11 ■ 1111 > 11 rllIl 11111111111 P p-rTT l ■ I > 1 I ‘ I ‘ I ‘ ‘ I ‘ ‘ ‘ I ' niz-> 2030405060 70 8090 100110120130140150160170180190200210 5.00 5.20 5.40 5.60 5.80

11602.D 052202.M Thu May 30 10:38:12 2002 Page 12

NYC-WTC_000013937

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