GCMS analysis results for sample AE08251, April 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08251.D Vial: 9 Acq On : 17 Apr 2002 4:02 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 11 N-(2-Acetylcyclopentylidene... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.47 0.54 ug/L 501884 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-(2-Acetylcyclopentylidene)cycl... 207 C13H21NO 1000100-48-5 9 2 Dodecahydropyrido[1,2-b]isoquino... 207 C13H21NO 1000195-30-7 5 3 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 4 5-Methyl-2-phenylindolizine 207 C15H13N 036944-99-7 5 Abundance Scan 406 (5.465 min) 08251 D (-387) (-) m/z 40.00 100.00% 4b 207

5000

84 96 I49 5.20 5.40 5.60 5.80

Tl/Z-> 0+I" 20 -1— 40 60 T" 80 100 120 140 160 180 200 m/z 207.00 89.33% Abundance #84801: N-(2-Acetylcyclopentylidene)cyclohexylamine 207

164 124 41 5000 55 5 20 540 5.60 5 80 82 97 110 150 67 192 m/z 96.10 24.39% - 136 । 178 0+ Kr — I ,l , | . n/z— > 20 40 60 80 100 120 140 160 180 :200 Abundance #84738: Dodecahydropyrido[1,2-b]isoquinolin-6-one 207 84 ' 1 i 1 1 5 20 5 40 5 60 5 80 5000 m/z 83.90 21.14% 97 192

29 41 55 67 109 125 138 152 164 178 MpMAuWwsMtrun n/z-> 0+ 20 — 40 60 80 100 120 pll , h,. 140 H 160 A' m 180 • I 1 200 Abundance #84862 Pyrido[2.3-d]pyrimidine, 4-phenyl- 207 5.20 5.40 5.60 5.80 m/z 208.00 17.68%

5000 179 77 103

n/Z—> 0 -A ----- 20 40 60 80 8+— 100 127

120 — 140 160 180 200 5.20 5.40 5.60 5.80

08251.D 041702SCAN.M Thu Apr 18 09:12:16 2002 Page 16

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