GCMS data file header for May 24-28, 2002

NYC 9/11 Public Portal Document Llorary aearen compound Report

Data File : C:\MSDCHEM\l\DATA\052802\524LB.D Vial: 3 Acq On : 28 May 2002 3:56 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan ** Library : C:\DATABASE\NIST98.L Peak Number 15 3,5-Dimethyl-4-iodoisoxazole Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 36.57 0.45 ug/L 235074 Perylene-d12 34.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,5-Dimethyl-4-iodoisoxazole 223 C5H6INO 061314-41-8 9 2 6-Bromoquinaldine 221 C10H8BrN 000877-42-9/5 3 5,5-Dimethyl-2-(dimethylamino)-1... 209 C7H16NO2PS1 015905-28-9/ 5 4 2-Phenyl-2-(phenylcarbamoyl)inda... 341 C22H15NO3 088702-68-/ 3 Abundance Scan 5700 (36.570 min): 524LB.D (-5686) (-) m/z 429.00 109-00% 133 191 223 281 341 419

5000- 96

• i ■ • TIT ■ ■ i ■ ■ ■ ■ i ■ 3620 36.40 36.60 36.80 37.00 44 ....................................... — 0-r * • 1 ‘ * m/z 281.00 94.92% miz-> 0 50 100 150 200 250. 300 350 400 Abundance #88246:3,5-Dimethyl-4-iodoisoxazole 43 223

5000 96 181 36.20 36.40 36.60 36.80 37.00 m/z 341.00 91.88% 127 154 0-T J4aL f ■ ky 1, -------------- miz-> o 50 100 150 200 250 300 350 400 Abundance #88369:6-Bromoquinaldine 223 3620 36.40 36.60 36.80 37.00 115 m/z 190.90 90.86% 5000 142

50 75 169 195, A 0 4, 274 +1/h,4 4 1 1 n/z-> 0 50 100 150 200 250 300 350 400 Abundance #6161:5,5-Dimethyl-2-(dimethyiarnino)-1,3,2-dioxaphosphori... JUL — 11 i ' ■ 1’ 43 36.20 36.40 36.60 36.80 37.00 69 m/z 133.00 89.34% 133 209 5000 d

176 0-T I m/z—> 0 50 100 150 200 250 300 350 400 36.20 36.40 36.60 36.80 37.00

524LB.D 052202.M Thu May 30 10:44:19 2002 Page 18

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