GCMS analysis report sample AE09678, May 23, 2002

NYC 9/11 Public Portal Document Llbrary aearen compound Report

Data File : C:\MSDCHEM\1\DATA\052102\9678.D Vial: 16 Acq On : 22 May 2002 1:33 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 8 trans-2,3-Methylenedioxy-b-... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 5.38 0.56 ug/L 323681 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 trans-2,3-Methylenedioxy-b-methy... 207 C10H9NO4 086029-47-2 9 2 Vanadium, (.eta.7-cycloheptatrie... 207 C12H12V 012636-68-9/5 3 Propiolonitrile 51 C3HN 001070-71-9 5

A 4 trans-2,3-Methylenedioxy-b-methy... 207 C10H9NO4 086029-47/2 4 Abundance Scan 391 (5.377 min): 9678.D (-385) (-) m/z 207.00 100.00% 84 207 51

5000 191 38 96 133 5.00 5.20 5.40 5.60 5.80

niz-> 0- nnni 20 111 40 • > i > ' ■ > i । 60 80 100 120 140 160 180 200 m/z 84.00 83.11% Abundance #126466: trans-2,3-Methylenedioxy-b-methyl-b-nitrostyrene 77 103 147 207

51 5000 91 39 5.00 5.20 5.40 5.60 5.80 63 119 131 m/z 51.10 77.84% 160 179 0- * • i * * • * । • • * * i • • "I — miz-> 20 40 60 80 100 120 1.40 160 180 200 Abundance #126462: Vanadium, (.eta.7-cycloheptatrienylium)(.eta.5-2,... 207 ' i 1 ' ' ' i ■ ■ ■ 1 I ■ ■ ■ ■ i ' ■ ■ ■ i ■ 129 5.00 5.20 5.40 5.60 5.80 51 5000 116 m/z 191.00 28.78%

— 90 0-1 39 • • i 65 TIIITTTT 76 | r, 1 I' j । > > ■ । i i 140 1 • ■ ■ ■ I ■ ■ ■ ■ i ■ 181 n/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #12371: Propiolonitrile 51 5.00 5.20 5.40 5.60 5.80 m/z 95.90 21.89% 5000

12 25 38 0 . F 1 L... . — n/z-> 20 40 60 80 100 120 140 160 180 200 5.00 5.20 5.40 5.60 5.80

9678.D 052202.M Wed May 22 11:43:27 2002 Page 11

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