GCMS blank analysis for sample AE12163, May 2002

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Laboratory report documenting GCMS analysis of sample AE12163 conducted on May 29, 2002.

NYC-WTC_000013775–000013782

Folder label: “GCMS X 5/23/02 A 5/29/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAY2902\LB.D Vial: 3 Acq On : 29 May 2002 1:18 pm Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 29 14:10 2002 Quant Results File:„GCMS0528.RES *** Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 08:55:48 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 589862 40.00 ug/1 -0.07 10) Naphthalene-d8 15.70 136 2348221 40.00 ug/1 -0.10 17) Acenaphthene-dl0 20.99 164 1110059 40.00 ug/1 -0.09 30) Phenanthrene-diO 25.43 188 1709208 40.00 ug/1 -0.11 38) Chrysene-dl2 33.47 240 999919 40.00 ug/1 -0.14 44) Perylene-dl2 37.66 264 624389 40.00 ug/,1 -0.15

System Monitoring Compounds 28) TCMX 23.13 209 220459 28.77 ug/L -0.10 Spiked Amount 40.000 Recovery 71.93% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 11.98 146 469 N.D. 5) 1,4-Dichlorobenzene 12.11 146 216 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'- oxybis (1 - Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 13.48 117 382 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 15.58 180 202 N.D. 15) Naphthalene 15.75 128 775 N.D. 16) Hexachiorobutadiene 16.30 225 516 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.27 165 101 N.D. 25) Diethylphthalate 22.48 149 275 N.D. 26) 4-Chlorophenylphenylether 23.12 204 1415 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.12 168 789 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.42 178 1113 N.D. (#) = qualifier out of range (m) = manual integration LB.D GCMS0528.M Wed May 29 14:10:28 2002 Page 1

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