GCMS analysis results for sample AE12278, June 2002

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Laboratory report documenting GCMS analysis of sample AE12278 conducted on June 3, 2002.

NYC-WTC_000013720–000013729

Folder label: “GCMS X 5/23/02 A 5/30/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAY2902\12278.D Vial: 19 Acq On : 30 May 2002 5:00 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 30 10:31 2002 Quant Results File: GCMS0528.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 08:55:48 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.07 152 557907 40.00 ug/1 -0.08 10) Naphthalene-d8 15.70 136 2236378 40.00 ug/1 -0.10 17) Acenaphthene-diO 20.99 164 1071938 40.00 ug/1 -0.10 30) Phenanthrene-diO 25.43 188 1619755m 40.00 ug/1 -0.11 38) Chrysene-dl2 33.47 240 933482 40.00 ug/1 -0.14 44) Perylene-dl2 37.66 264 602319 40.00 ug/1 -0.15 System Monitoring Compounds 28) TCMX 23.13 209 227773 30.78 ug/L -0.10 Spiked Amount 40.000 Recovery 76.95%

Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 11.98 146 502 N.D. 5) 1,4-Dichlorobenzene 12.06 146 1089 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 13.47 117 263 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 15.59 180 219 N.D. 15) Naphthalene 15.75 128 1045 N.D. 16) Hexachlorobutadiene 16.30 225 410 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chioronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.48 149 1655 N.D. 26) 4-Chlorophenylphenylether 23.13 204 1420 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 0.00 178 0 N.D. d (#) = qualifier out of range (m) = manual integration 12278.D GCMS0528.M Thu May 30 10:32:12 2002 Page 1

NYC-WTC_000013722

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NYC-WTC_000013730

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