Gas chromatography-mass spectrometry Method 508 analysis worksheet with sample extraction parameters and measurement data from May 23, 2002.
NYC-WTC_000013696–000013707Folder label: “GCMS X 5/23/02 A 5/30/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\MAY2902\LBA.D Vial: 16 Acq On : 30 May 2002 2:04 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 30 9:45 2002 Quant Results File: GCMS0528.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 08:55:48 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 580859 40.00 ug/1 -0.08 10) Naphthalene-d8 15.69 136 2313883 40.00 ug/1 -0.10 17) Acenaphthene-diO 20.99 164 1096689 40.00 ug/1 -0.10 30) Phenanthrene-diO 25.42 188 1692630 40.00 ug/1 -0.11 38) Chrysene-dl2 33.48 240 1004928 40.00 ug/1 -0.13 44) Perylene-dl2 37.65 264 644129 40.00 ug/1 -0.15
System Monitoring Compounds 28) TCMX 23.14 209 244575 32.30 ug/L -0.09 Spiked Amount 40.000 Recovery 80.75% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane o.ob 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.75 128 197 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.49 149 1053 N.D. 26) 4-Chlorophenylphenylether 23.13 204 1216 N.D. 27) Fluorene 0.00 166 0 N.D. 2 9) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.14 168 901 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.42 178 672 N.D. (#) = qualifier out of range (m) = manual integration LBA.D GCMS0528.M Thu May 30 09:46:16 2002 Page 1
NYC-WTC_000013699
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NYC-WTC_000014733
GCMS blank analysis report for sample AE12093 dated 05/31/2002 showing all measured organic compounds below minimum reporting limits (MRL) of 2.0 micrograms.
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Laboratory blank report for GCMS analysis of volatile organic compounds conducted on May 31, 2002.
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Laboratory report documenting GCMS analysis of sample AE12163 conducted on May 29, 2002.
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Laboratory blank report for GCMS analysis of volatile organic compounds conducted on May 31, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
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Laboratory report showing GCMS blank analysis results for volatile organic compounds in sample AE12535 on June 3-4, 2002.
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Laboratory report showing GCMS blank analysis for sample AE12152 with results below method detection limits.
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Laboratory report showing blank analysis results for volatile organic compounds in sample AE05750 from April 2002.
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Laboratory data sheet recording GCMS blank analysis parameters for sample AE09579 conducted on May 8, 2002.
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Laboratory report documenting a blank sample analysis for GCMS testing of volatile organic compounds in April 2002.
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Laboratory report showing GCMS blank analysis results for sample AE01156 conducted on March 25, 2002, with compound detection limits.
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Blank run report confirming absence of target compounds below detection limits for sample AE06991 on April 6, 2002.
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Laboratory report of a GC/MS blank run analyzing volatile organic compounds with results below detection limits in May 2002.
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NYC-WTC_000013695
Department of Environmental Protection record of GCMS results generated in late May 2002.
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NYC-WTC_000013708
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NYC-WTC_000013730
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