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GCMS Method 508 analysis worksheet, May 2002

Machine-extracted title · confidence 72%

Gas chromatography-mass spectrometry Method 508 analysis worksheet with sample extraction parameters and measurement data from May 23, 2002.

NYC-WTC_000013696–000013707

Folder label: “GCMS X 5/23/02 A 5/30/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\MAY2902\LBA.D Vial: 16 Acq On : 30 May 2002 2:04 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 30 9:45 2002 Quant Results File: GCMS0528.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 08:55:48 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Compound R.T. QIon Response Cone Unit Qvalue 35) Anthracene 25.42 178 672 N.D. 36) Di-n-butylphthalate 27.41 149 35747 0.64 ug/1 99 37) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.47 228 2532 N.D. 42) Bis(2-ethylhexyl)phthalate 33.71 149 3266 N.D. 43) Chrysene 33.47 228 2532 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.66 252 2644 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LBA.D GCMS0528.M Thu May 30 09:46:17 2002 Page 2

NYC-WTC_000013700

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NYC-WTC_000013700Source: NYC Law Department, mirrored locally

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