GCMS calibration table data, sample AE09677, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0 602\9677.D Vial: 20 Acq On 7 May 2002 10:54 am Operator: Sample GC/MS SCAN 4/25 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.16 10.80 ug/1 1004030 1,4-Dichlorobenzene-d4 12.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 CH2=CIK:H2C(O)OCH3 100 C5H802 003724-55-8 9 3 Acetone 58 C3H60 000067-64-1 7 4 Butane 58 C4H10 000106-97-8 5 Abundance • Scan 340 (8.159 min): 9677.D (-) m/z 43.05 100.00% 43

5000 59

101 7.80 8.00 8.20 8.40 8.60

niz-> 04 ........................ 38 1 +53+ ■ ■ i ' • ‘ ■ i ■ ■ ■ ■ i ■ ■ < i j ■ 10 20 30 40 50 60 69 I ■ • • ■T 1 ■ 1 ■ i 70 80 83 - 90 100 110 m/z 59.10 41.73% Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 . ,-r । i ... । . 59 7.80 8.00 8.20 8.40 8.60 m/ Z 58.10 16.77%

miz->10 20 27 I I 30 I +49 40 50 1‘ 60 83 ——————— 70 80 90 + 101

100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 • i ‘ * t I l < 7.80 8.00 8.20 8.40 8.60 5000 13.28%

-111111138/ ..... ”.... 7. 100 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone >43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 7.07%

5000 15 58

/z-> 27 । । —l । , 11l, , , , ) *rl '' 10 20 30 40 50 i • ' ' ' i ■ ' ■ ■ i ‘ 60 70 80 ' i ■ ' ■ ' i ■ ■ ■ ■ i ■ 90 100 110 .. .... IL..... 1 ' \ —Opgn i" r । । ii । Q - cram 7.80 8.00 8.20 8.40 8.60

9677.D GCMS0501.M Thu May 09 11:25:19 2002 Page 1

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