Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.
NYC-WTC_000012751–000012778Folder label: “GCMS X 5-21-02 A 5-22-02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052202\521LB.D Vial: 3 Acq On : 22 May 2002 3:27 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 6-Bromoquinaldine Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 34.86 0.57 ug/L 226501 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 6-Bromoquinaldine 221 C10H8BrN 000877-42-9 9 2 2-(2-Hydroxybenzylidene-amino)-3... 356 C23H20N2O2 1000147-86-3 9 3 Methanimidamide, N,N-dimethyl-N'... 221 C11H15N3O2 022259-30-9 9 4 Bis[4-(2,5-dimethyl-l-pyrrolyl)p... 356 C24H24N2O 1000225-09-3 7 Abundance Scan 5408 (34.854 min): 521 LB.D (-5406) (-) m/z 207.05 100.00% 207 356 149 44 _ 73 96 283 5000 260
.AA 34.60 34.80 35.00 35.20
miz-> 0— 0 -nodaoi 50 100 150 200 250 300 || 350 1 400 429 m/z 221.10 94.14% Abundance #88369:6-Bromoquinaldine 223
115 5000 142 34.60 34.80 35.00 35.20 m/z 223.10 91.80% 50 75 0- 4 .274 ’ ll 41 fi 11 169, 195, ... miz-> 0 50 100 150 200 250 300 400 350 Abundance #87998:2-(2-Hydroxybenzylidene-amino)-3-(N-me-N-(O-tolyl)... 221 356 7 34.60 34.80 35.00 35.20 5000 m/z 356.10 77.34% 91 65 , 134 178 .249
miz-> 0-T 0 -L, 1 I 1 i 50 100 150 200 250 1 300 350 400 Abundance #87896: Methanimidamide, N,N-dimethyl-N‘-[3-II(methylamino... ■ • i ■ ■ • ■ i 44 163 2211 34.60 34.80 35.00 35.20 m/z 96.20 71.09% 122 5000 65 93
| i . .4 J.s 1, Jr 183‘ i ‘ f ' ' i ‘ 0 1 ‘ ' i ‘ 1 ■ ' i ■ ■ ■ ■ i • ■
mfz-> 0 50 100 150 200 250 300 350 400 34.60 34.80 35.00 35.20
521LB.D 052202.M Tue May 28 11:58:06 2002 Page 16
NYC-WTC_000012770
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NYC-WTC_000012823
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015496
Laboratory report showing non-detect levels of volatile organic compounds in a GCMS blank sample analyzed on June 5, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013524
Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013574
Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013418
Quality control document showing GCMS blank results for multiple volatile organic compounds analyzed on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012937
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025054
Laboratory report showing GCMS blank analysis for sample AE11379 conducted on May 21, 2002, with results below minimum reporting levels.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000012748
Department of Environmental Protection record of GCMS results generated in late May 2002.
Filed in the same folder
NYC-WTC_000012749
Administrative log recording sample identification, drip rates, and processing details for a GCMS batch.
Filed in the same folder
NYC-WTC_000012779
Calibration data for gas chromatography-mass spectrometry analysis of semivolatile organic compounds recorded on May 28, 2002.
Filed in the same folder
NYC-WTC_000012783
Reference standard analysis data for gas chromatography-mass spectrometry testing of semivolatile organic compounds on May 28, 2002.
Filed in the same folder
NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
Filed in the same folder