GCMS data file header for May 24-28, 2002

NYC 9/11 Public Portal Document Library Search compound Report

Data File : C:\MSDCHEM\l\DATA\052802\524LB.D Vial: 3 Acq On : 28 May 2002 3:56 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) : 508 Modified GC/MS scan *** Title Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Malonic acid, 2-(2,3-dihydr... Concentration Rank. 10 R.T. EstConc Area Relative to ISTD R.T. 35.37 0.41 ug/L 217617 Perylene-d12 34.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Malonic acid, 2-(2,3-dihydrobenz... 266 C13H1406 1000158-50/7 12 2 Pentasiloxane, dodecamethyl- 384 C12H3604Si5 000141-63/9 10 3 1,3-Benzodioxole, 5-[3-acetamino... 221 C12H15NO3 1000124-33-0 9 4 3H-V-Triazolo[4,5-d] pyrimidine, 7.. . 221 C9H11N5S 1000147-85-7 9 Abundance Scan 5496 (35.371 min): 524LB.D (-5490) (-) m/z 147.00 00.00% 73 147 221

5000 281 355 429 1 . A......... ' 1 ‘ 1 1 1 1 1 1 A 35.00 35.20 35.40 35.60 35.80

mfe-> 0- 44 ■ 1 50 At 1911 100 150 200 250 300 III, 350 IJ 400 X m/z 221.00 91.32% Abundance #66292: Malonic acid, 2-(2,3-dihydrobenzo[b]furan-5-yl)-2-... 147

5000 207 J,,, 11*** I* 35.00 35.20 35.40 35.60 35.801 65 91 119 m/z 73.10 88.51% 266

miz-> 0- 3950—111184 100 150 177 200 233 250 ■ ‘ i 1 [ 300 • ■ ■ i ■ ■ ■ ■ 350 i • ' ■ ■ 400 i ■

Abundance #115143: Pentasiloxane, dodecamethyl- 73 147 281 MnnbymnAanptme-ht"ny 35.00 35.20 35.40 35.60 35.80 5000 m/z 207.00 48.76% 369 207 0- —Lr + - 93 117 .177.1.29 4, 45 niz-> 50 100 150 200 250 300 Abundance #87894:1,3-Benzodioxole, 5-[3-acetaminopropyl]- 221 35.00 35.20 35.40 35.60 35.80 m/z 281.05 37.72% 135 162 43 73 5000

I 104 ।

0 1,4.419 J 92, m/z-> 50 100 150 200 250 300 350 400 35.00 35.20 35.40 35.60 35.80

524LB.D 052202.M Thu May 30 10:44:18 2002 Page 16

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