GCMS pesticide analysis results, sample AE11573, May-June 2002

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Data File : C:\MSDCHEM\1\DATA\052902\11311RR.D Vial: 16 . Acq On : 29 May 2002 2:39 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 RE-EXTD 5/23/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L *** ********************************************************************* Peak Number 11 Heptadecane $$ n-Heptadecan ... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

22.72 0.06 ug/L 94191 Phenanthrene d-10 22.51

Hit# of 5 Tentative ID MW MolForm CAS# Qual l Heptadecane $$ n-Heptadecane $$ ... 240 C17H36 000629-78-7 91 2 Octacosane 394 C28H58 000630-02-4 86 3 Nonacosane 408 C29H60 000630-03-5 86 4 Octacosane (CAS) $$ n-Octacosane 394 C28H58 000630-02-4 86 Abundance Scan 1284 (22.722 min): 11311RR.D (-) m/z 57.10 100.00% 57

85 5000

(113 141 MAMss 22.40 22.60 22.80 23.00 18—UM 1 0 m/z 71.05 85.54% m/z-> 50 100 150 200 250 300 350 400 ... Abundance #174546: Heptadecane $$ n-Heptadecane $3 Normal-heptadecane 57

85 5000 22.40 22.60 22.80 23.00 m/z 85.10 57.33% 29 11131,141.169 197 2° 0- 8)7 100 150 200 250 300 350 400 ws MMAA m/z-> Abundance #329267: Octacosane 57

22.40 22.60 22.80 23.00 5000 m/z 55.10 29.40% 85

29 ! i 113 141 m/z-> Abundance 0- -44++4,44,4+ 169 197 225 253 281 309 337 365 394 50

57 100 150 200 250 #337000: Nonacosane 300 350 400 MMla 22.40 22.60 22*80 23.00 ~ m/z 99.20 23.71%

5000 85

m/z—> 0J 24 50 113 4-1 1 J. 141,169,197 225 253 281 309 337 365 1“1f1n 1 14 di* f 41 TTi* r-, i .-.i f i. ■ 1 7 T 100 150 200 250 300 350 400 408

1311RR.D 052802.M Mon Jun 03 15:50:26 2002 Page 13

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