GCMS laboratory blank results, sample AE11555, May 23-29, 2002

NYC 9/11 Public Portal Document Liprary searcn compound Report

Data File : C:\MSDCHEM\1\DATA\052902\LBB0529.D Vial: 15 Acq On : 29 May 2002 1:53 pm Operator: Bohlk / Inst 213 ‘ Sample : LB 5/23/02 Inst : Instrumen Mise : Multipir: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ***

Peak Number 2 Dodecane, 1-iodo- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 14.75 0.08 ug/L 111118 Acenaphthene-diO 18.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dodecane, 1-iodo- 296 C12H25I 004292-19-7 64 2 Eicosane 282 C20H42 000112-95-8 64 3 Hexane, 3,3-dimethyl- $$ 3,3-Dim— 114 C8H18 000563-16-6 64 4 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 64 Abundance Scan 405 (14.749 mln): LBB0529.D (-) m/z 71.10 100.00% 71

5000

5.5 99 127 EE AAA4 14.40 14.60 14.80 15.00 m/z 57.10 78.32% m/z-> 0- ag0uingnapel — T’’t"13TT’1rt2m523’1"911191"’192030"19218T 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #244391: Dodecane, 1-iodo­ 57

............. 5000 85 41 14.40 14.60 14.80 15.00 m/z 85.10 66.83% , 113 155

mlz-> 0^ i1’J81 -7.1,183. I“ I 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #228992: Eicosane 57

-4— AALAAA4 14.40 14.60 14.80 15.00 5000 m/z 55.10 20.54% 85 41

+444.413.141 0- ' I >' TTT‘ 282 169 TIUIII TTTTTT T "i” miz-> Abundance 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 #15678: Hexane, 3,3-dimethyl- $$ 3,3-Dimethylhexane 43 AA 14.40 14.60 14.80 15.00 m/z 99.10 17.98%

5000 71

27

m/z-> 2 , 0 ■ i • ■ ■’ i •'A. ■•••I 1, 11 ■ 1. 11 > 1.1 > 11.........j 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 14.40 14.60 14.80 15.00 1IT

1BB0529.D 052802.M Mon Jun 03 15:47:21 2002 Page 4

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